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Beilstein J. Org. Chem. 2012, 8, 890–896, doi:10.3762/bjoc.8.101
Graphical Abstract
Figure 1: Structures of azobenzene thioesters, Nα-ligation auxiliaries and peptides for the application in li...
Scheme 1: Structural differences between the trans- and the cis-state of azopeptides with a SKV PDZ binding m...
Figure 2: Structure of the glycine-linked auxiliary conjugates 7 and 8.
Scheme 2: Solid-phase synthesis of the ligation-mediating peptides 3–5.
Scheme 3: Reduction of the diazene unit of 4,4'-AMPB thioesters and peptides during aliphatic thiol-based Nα-...
Scheme 4: Synthesis of the azopeptides 16/17 by final TFA cleavage of the Boc-protecting groups, and of the a...